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In brief, 10 mL of wastewater sample containing the surrogate at 0.5 μg·mL −1 was placed in an 18 mm vial with adding 2.6 g of sodium chloride. Then, the vials were sealed with a septum cap and pre-heated at 65 °C (3 min); Afterward, a 75 μm carboxen/polydimethylsiloxane (CAR/PDMS) fiber was placed into the vial headspace, and the